Fe^II(N(TMS)₂)₂(Pcycyclohexyl₃)

Base Information

• Chemical Name: Fe^II(N(TMS)₂)₂(Pcycyclohexyl₃)
• CAS No.: 1334702-01-0
• Molecular Formula: C₃₀H₆₉FeN₂PSi₄
• Molecular Weight: 657.054
• Mol file: 1334702-01-0.mol

Synonyms:

Chemical Property of Fe^II(N(TMS)₂)₂(Pcycyclohexyl₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Fe^II(N(TMS)₂)₂(Pcycyclohexyl₃)

There total 3 articles about Fe^II(N(TMS)₂)₂(Pcycyclohexyl₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

[Fe{N(SiMe3)2}2]2 (133984-08-4) + tricyclohexylphosphine (2622-14-2) → FeII(N(TMS)2)2(Pcycyclohexyl3) (1334702-01-0)

Guidance literature:

In n-heptane; Heating; Inert atmosphere;

DOI:10.1021/ic401677j

Reference yield:

potassium hexamethylsilazane (40949-94-8) + iron(II) chloride + tricyclohexylphosphine (2622-14-2) → FeII(N(TMS)2)2(Pcycyclohexyl3) (1334702-01-0)

Guidance literature:

In tetrahydrofuran; reaction of iron compd. with phosphine deriv. in THF, addn. of potassiumamide deriv. at -25°C;

DOI:10.1021/ja203845x

Reference yield:

iron(II) bis(trimethylsilyl)amide (14760-22-6) + tricyclohexylphosphine (2622-14-2) → FeII(N(TMS)2)2(Pcycyclohexyl3) (1334702-01-0)

Guidance literature:

In not given; (inert atm.); addn. of phosphine deriv. to iron compd.;

DOI:10.1021/ja210542r

upstream raw materials:

potassium hexamethylsilazane

tricyclohexylphosphine

iron(II) bis(trimethylsilyl)amide

[Fe{N(SiMe₃)₂}₂]₂