1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine

Base Information

Chemical Name:1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine
CAS No.:150107-62-3
Molecular Formula:C₂₆H₃₀N₂O₆
Molecular Weight:466.534
Hs Code.:

1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-<carbo(t-butyloxy)>methyl-hexahydro-1,5-diazepine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine

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Technology Process of 1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine

There total 3 articles about 1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143182-17-6
N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

: 150107-62-3
1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 5 percent Pd/C / methanol / 4 h / 2585.7 Torr / Ambient temperature

2: diphenylphosphoryl azide / dimethylformamide / 72 h / Ambient temperature

3: 1) KN(TMS)2, HMPA / 1) THF, -78 deg C, 20 min, 2) to r.t., 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; diphenylphosphoranyl azide; hydrogen; potassium hexamethylsilazane; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)90208-X

Reference yield:

: N-[2-(tert-Butoxycarbonylmethyl-amino)-ethyl]-N-phenyl-malonamic acid

: 150107-62-3
1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: diphenylphosphoryl azide / dimethylformamide / 72 h / Ambient temperature

2: 1) KN(TMS)2, HMPA / 1) THF, -78 deg C, 20 min, 2) to r.t., 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; diphenylphosphoranyl azide; potassium hexamethylsilazane; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)90208-X

Reference yield:

: 81867-37-0
benzyl iodoacetate

: 143148-29-2
1-Phenyl-2,4-dioxo-5-methyl-hexahydro-1,5-diazepine

: 150107-62-3
1-Phenyl-2,4-dioxo-3-(carbobenzyloxy)methyl-5-methyl-hexahydro-1,5-diazepine

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; Yield given. Multistep reaction; 1) THF, -78 deg C, 20 min, 2) to r.t., 2 h;
DOI:10.1016/S0040-4020(01)90208-X