C₂₉H₃₉BN₂O₃*ClH

Base Information

• Chemical Name: C₂₉H₃₉BN₂O₃*ClH
• CAS No.: 1426811-68-8
• Molecular Formula: C₂₉H₃₉BN₂O₃*ClH
• Molecular Weight: 510.912
• Mol file: 1426811-68-8.mol

Synonyms:

Chemical Property of C₂₉H₃₉BN₂O₃*ClH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₉BN₂O₃*ClH

There total 6 articles about C₂₉H₃₉BN₂O₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H28BN3O2 (1426811-50-8) → C29H39BN2O3*ClH (1426811-68-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

1.2: Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / Inert atmosphere

3.1: hydrogenchloride / methanol / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1111/cbdd.12091

Reference yield:

C20H30BNO2*ClH (1426811-58-6) → C29H39BN2O3*ClH (1426811-68-8)

Guidance literature:

Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / Inert atmosphere

2: hydrogenchloride / methanol / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;

DOI:10.1111/cbdd.12091

Reference yield:

(-)-pinanediol bromomethaneboronate (852509-27-4) → C29H39BN2O3*ClH (1426811-68-8)

Guidance literature:

Multi-step reaction with 6 steps

1.1: sodium azide; tetrabutylammomium bromide / dichloromethane; water / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -100 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: zinc(II) chloride / tetrahydrofuran / -78 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

4.2: Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / Inert atmosphere

6.1: hydrogenchloride / methanol / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; sodium azide; tetrabutylammomium bromide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1111/cbdd.12091

upstream raw materials:

C₂₀H₂₈BN₃O₂

C₂₀H₃₀BNO₂*ClH

(-)-pinanediol bromomethaneboronate

C₃₄H₄₇BN₂O₅

Downstream raw materials:

tlo_245_481