C₆₀H₁₀₂O₁₃Si₂

Base Information

Chemical Name:C₆₀H₁₀₂O₁₃Si₂
CAS No.:1331882-39-3
Molecular Formula:C₆₀H₁₀₂O₁₃Si₂
Molecular Weight:1087.63
Hs Code.:

C<sub>60</sub>H<sub>102</sub>O<sub>13</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₆₀H₁₀₂O₁₃Si₂

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Technology Process of C₆₀H₁₀₂O₁₃Si₂

There total 15 articles about C₆₀H₁₀₂O₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1331883-18-1
C₂₆H₃₅IO₄

: C₄₀H₇₉BO₁₁Si₂

: 1331882-39-3
C₆₀H₁₀₂O₁₃Si₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide; In tetrahydrofuran; water; at 25 ℃; for 1h;
DOI:10.1021/jo200934w

Reference yield:

: (2E,4E)-2,4-dimethyl-6-oxo-hexa-2,4-dienoic acid tert-butyl ester

: 1331882-39-3
C₆₀H₁₀₂O₁₃Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate / methanol / 0.33 h / 0 - 25 °C

2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.67 h / 25 °C

3.1: toluene / 17 h / Reflux

4.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C

4.2: 3 h / -78 - 25 °C

5.1: ammonium fluoride / methanol / 15 h / 60 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -60 °C

6.2: 1.5 h / -78 - 0 °C

7.1: chromium dichloride / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide / tetrahydrofuran; water / 1 h / 25 °C

With chromium dichloride; ammonium fluoride; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; carbon tetrabromide; thallium (I) ethoxide; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; toluene; 2.1: Appel reaction / 4.2: Horner-Wadsworth-Emmons olefination / 6.1: Swern oxidation / 6.2: Swern oxidation / 7.1: Takai olefination / 8.1: Suzuki-Miyaura coupling;
DOI:10.1021/jo200934w

Reference yield:

: 1331882-71-3
C₁₂H₁₉BrO₂

: 1331882-39-3
C₆₀H₁₀₂O₁₃Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene / 17 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C

2.2: 3 h / -78 - 25 °C

3.1: ammonium fluoride / methanol / 15 h / 60 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -60 °C

4.2: 1.5 h / -78 - 0 °C

5.1: chromium dichloride / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide / tetrahydrofuran; water / 1 h / 25 °C

With chromium dichloride; ammonium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; thallium (I) ethoxide; dimethyl sulfoxide; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; toluene; 2.2: Horner-Wadsworth-Emmons olefination / 4.1: Swern oxidation / 4.2: Swern oxidation / 5.1: Takai olefination / 6.1: Suzuki-Miyaura coupling;
DOI:10.1021/jo200934w