Technology Process of C24H26N4O4
There total 4 articles about C24H26N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
cesiumhydroxide monohydrate; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide;
In
dichloromethane;
at -30 ℃;
enantioselective reaction;
DOI:10.1016/j.bmcl.2013.02.039
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide; water / Reflux
2: sodium nitrite; tetrafluoroboric acid / water
3: dimethylsulfide borane complex / tetrahydrofuran / -20 °C / Reflux
4: carbon tetrabromide; triphenylphosphine / dichloromethane
5: O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; cesiumhydroxide monohydrate / dichloromethane / -30 °C
With
tetrafluoroboric acid; cesiumhydroxide monohydrate; carbon tetrabromide; dimethylsulfide borane complex; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; water; triphenylphosphine; sodium hydroxide; sodium nitrite;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.02.039
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium nitrite; tetrafluoroboric acid / water
2: dimethylsulfide borane complex / tetrahydrofuran / -20 °C / Reflux
3: carbon tetrabromide; triphenylphosphine / dichloromethane
4: O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; cesiumhydroxide monohydrate / dichloromethane / -30 °C
With
tetrafluoroboric acid; cesiumhydroxide monohydrate; carbon tetrabromide; dimethylsulfide borane complex; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; triphenylphosphine; sodium nitrite;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.02.039