[Ir(ppy)2(phenyl-C₁₃H₇N₄)](hexafluorophosphate)

Base Information

• Chemical Name: [Ir(ppy)2(phenyl-C₁₃H₇N₄)](hexafluorophosphate)
• CAS No.: 960378-74-9
• Molecular Formula: C₄₁H₂₈IrN₆*F₆P
• Molecular Weight: 941.898

Synonyms:

Chemical Property of [Ir(ppy)2(phenyl-C₁₃H₇N₄)](hexafluorophosphate)

Chemical Property:

Purity/Quality:

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Technology Process of [Ir(ppy)2(phenyl-C₁₃H₇N₄)](hexafluorophosphate)

There total 2 articles about [Ir(ppy)2(phenyl-C₁₃H₇N₄)](hexafluorophosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[iridium(III)(μ-chloro)(2-phenylpyridine)2]2 + ammonium hexafluorophosphate + 2-phenyl-1H-imidazo[4,5-f ][1,10]phenanthroline (171565-44-9) → [Ir(ppy)2(phenyl-C13H7N4)](hexafluorophosphate) (960378-74-9)

Guidance literature:

[iridium(III)(μ-chloro)(2-phenylpyridine)2]2; 2-phenyl-1H-imidazo[4,5-f ][1,10]phenanthroline; In methanol; dichloromethane; for 4h; Inert atmosphere; Reflux; Darkness;

ammonium hexafluorophosphate; In methanol; dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/c9cc04871e

Reference yield: 60.5%

ammonium hexafluorophosphate + [iridium(III)(μ-chloro)(2-phenylpyridine)2]2 + 2-phenyl-1H-imidazo[4,5-f ][1,10]phenanthroline (171565-44-9) → [Ir(ppy)2(phenyl-C13H7N4)](hexafluorophosphate) (960378-74-9)

Guidance literature:

In methanol; dichloromethane; (Ir(ppy)2Cl)2 (0.1 mmol) and C6H5C13H7N4 (0.087 mmol) dissolved in CH2Cl2/MeOH (2:1, v/v), heated at reflux for 5-6 h under Ar, cooled to room temp., NH4PF6 (10-fold excess) added, stirred for 15 min; filtered, soln. concd. to dryness under vac., chromd. (silica gel, CH2Cl2/MeOH (10:1)); elem. anal.;

DOI:10.1002/ejic.201100501

upstream raw materials:

2-phenyl-1H-imidazo[4,5-f ][1,10]phenanthroline

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