Technology Process of C24H34N2O6Si
There total 11 articles about C24H34N2O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane
2: 1H-imidazole / N,N-dimethyl-formamide
With
1H-imidazole; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.012
- Guidance literature:
-
Multi-step reaction with 9 steps
2: sodium hydride / N,N-dimethyl-formamide
3: sulfuric acid; acetic acid
4: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate
5: tetrabutyl ammonium fluoride / tetrahydrofuran
6: pyridine
7: sodium hydroxide / 1,4-dioxane; water
8: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane
9: 1H-imidazole / N,N-dimethyl-formamide
With
pyridine; 1H-imidazole; N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
1: Grignard reaction / 4: Vorbruggen reaction;
DOI:10.1016/j.bmcl.2011.11.012
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / 1,4-dioxane; water
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane
3: 1H-imidazole / N,N-dimethyl-formamide
With
1H-imidazole; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.012
