Technology Process of 4-(3,4-dimethoxybenzylideneamino)naphthalene-1,2-dione
There total 3 articles about 4-(3,4-dimethoxybenzylideneamino)naphthalene-1,2-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / water; acetic acid / 2 h / 40 °C
2: acetic acid / ethanol; methanol / Reflux
With
sodium azide; acetic acid;
In
methanol; ethanol; water; acetic acid;
DOI:10.1007/s00044-012-0150-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium dithionite / 40 - 50 °C
2: iron(III) chloride; hydrogenchloride / Cooling with ice
3: sodium azide / water; acetic acid / 2 h / 40 °C
4: acetic acid / ethanol; methanol / Reflux
With
hydrogenchloride; iron(III) chloride; sodium azide; sodium dithionite; acetic acid;
In
methanol; ethanol; water; acetic acid;
DOI:10.1007/s00044-012-0150-7
- Guidance literature:
-
Multi-step reaction with 3 steps
1: iron(III) chloride; hydrogenchloride / Cooling with ice
2: sodium azide / water; acetic acid / 2 h / 40 °C
3: acetic acid / ethanol; methanol / Reflux
With
hydrogenchloride; iron(III) chloride; sodium azide; acetic acid;
In
methanol; ethanol; water; acetic acid;
DOI:10.1007/s00044-012-0150-7
