C₄₈H₅₄O₉

Base Information

Chemical Name:C₄₈H₅₄O₉
CAS No.:1449216-24-3
Molecular Formula:C₄₈H₅₄O₉
Molecular Weight:774.951
Hs Code.:

C<sub>48</sub>H<sub>54</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₄₈H₅₄O₉

Chemical Property:

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Technology Process of C₄₈H₅₄O₉

There total 15 articles about C₄₈H₅₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449216-21-0
C₂₇H₃₆O₈

: 1449216-22-1
C₃₉H₃₄O₂P⁽¹⁺⁾*Br^(1-)

: 1449216-24-3
C₄₈H₅₄O₉

: 1449216-26-5
C₄₈H₅₄O₉

Guidance literature:: C₃₉H₃₄O₂P⁽¹⁺⁾*Br^(1-); With n-butyllithium; In tetrahydrofuran; hexane; at 4 ℃; for 0.5h;

C₂₇H₃₆O₈; In tetrahydrofuran; hexane; at -78 - -10 ℃; for 3h; Overall yield = 41 %; Overall yield = 1.1 mg;
DOI:10.3987/COM-12-S(N)8

Reference yield:

: 1449216-13-0
C₃₆H₅₆O₄S₂Si

: 1449216-24-3
C₄₈H₅₄O₉

: 1449216-26-5
C₄₈H₅₄O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.1: silver(l) oxide; titanium tetrachloride; titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane; diethyl ether / 21 h / -15 - 4 °C / Inert atmosphere

3.1: acetic acid / tetrahydrofuran; water / 0.83 h / 55 °C

4.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 0.75 h / 4 °C

5.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 2 h / 20 °C

5.2: 1.5 h / 20 - 50 °C

6.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 1 h / 20 °C / pH 7.2

7.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 11.5 h / 4 °C

8.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 3 h / 20 °C

8.2: 5 h / 4 - 20 °C

9.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.67 h / 20 °C / Molecular sieve

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 4 °C

10.2: 3 h / -78 - -10 °C

With pyridine; titanium(IV) isopropylate; potassium permanganate; sodium periodate; n-butyllithium; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 1.1: |Ley Oxidation / 8.2: |Yamaguchi Lactonization;
DOI:10.3987/COM-12-S(N)8

Reference yield:

: C₃₆H₅₄O₄S₂Si

: 1449216-24-3
C₄₈H₅₄O₉

: 1449216-26-5
C₄₈H₅₄O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: silver(l) oxide; titanium tetrachloride; titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane; diethyl ether / 21 h / -15 - 4 °C / Inert atmosphere

2.1: acetic acid / tetrahydrofuran; water / 0.83 h / 55 °C

3.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 0.75 h / 4 °C

4.1: zinc(II) chloride / dichloromethane / 0.5 h / 20 °C

5.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 2 h / 20 °C

5.2: 1.5 h / 20 - 50 °C

6.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 1 h / 20 °C / pH 7.2

7.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 11.5 h / 4 °C

8.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 3 h / 20 °C

8.2: 5 h / 4 - 20 °C

9.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.67 h / 20 °C / Molecular sieve

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 4 °C

10.2: 3 h / -78 - -10 °C

With pyridine; titanium(IV) isopropylate; potassium permanganate; sodium periodate; n-butyllithium; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; zinc(II) chloride; silver(l) oxide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 8.2: |Yamaguchi Lactonization;
DOI:10.3987/COM-12-S(N)8