C₁₁H₁₆O₃S

Base Information

• Chemical Name: C₁₁H₁₆O₃S
• CAS No.: 1321603-31-9
• Molecular Formula: C₁₁H₁₆O₃S
• Molecular Weight: 228.312

Synonyms:

Chemical Property of C₁₁H₁₆O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₁H₁₆O₃S

There total 1 articles about C₁₁H₁₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-((4-methoxybenzyloxy)methyl)oxirane (108836-41-5) → C11H16O3S (1321603-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium thioacetate / dichloromethane / Inert atmosphere

2: methanol; sodium methylate / Inert atmosphere

With methanol; sodium methylate; potassium thioacetate; In dichloromethane;

DOI:10.1016/j.bmcl.2011.05.083

Reference yield:

C11H16O3S (1321603-31-9) → C12H17O5PS (1321603-33-1)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / Inert atmosphere

2: 2,6-dimethylpyridine / tetrahydrofuran; toluene / Inert atmosphere

With 2,6-dimethylpyridine; In tetrahydrofuran; toluene;

DOI:10.1016/j.bmcl.2011.05.083

Reference yield:

C11H16O3S (1321603-31-9) → C13H21O6PS

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / Inert atmosphere

2: 2,6-dimethylpyridine / tetrahydrofuran; toluene / Inert atmosphere

3: palladium on carbon; hydrogen / methanol / 20 °C

With 2,6-dimethylpyridine; palladium on carbon; hydrogen; In tetrahydrofuran; methanol; toluene;

DOI:10.1016/j.bmcl.2011.05.083

upstream raw materials:

2-((4-methoxybenzyloxy)methyl)oxirane

Downstream raw materials:

C₁₂H₁₇O₅PS

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