[Ni(1,3-bis(4-pyridyl)propane)(H₂O)][trimesic acid^(2-)]

Base Information

• Chemical Name: [Ni(1,3-bis(4-pyridyl)propane)(H₂O)][trimesic acid^(2-)]
• CAS No.: 1174064-14-2
• Molecular Formula: C₉H₄O₆*C₁₃H₁₄N₂*H₂O*Ni
• Molecular Weight: 483.1
• Mol file: 1174064-14-2.mol

Synonyms:

Chemical Property of [Ni(1,3-bis(4-pyridyl)propane)(H₂O)][trimesic acid^(2-)]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [Ni(1,3-bis(4-pyridyl)propane)(H₂O)][trimesic acid^(2-)]

There total 1 articles about [Ni(1,3-bis(4-pyridyl)propane)(H₂O)][trimesic acid^(2-)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1,3-di(4-pyridyl)propane (17252-51-6) + benzene-1,3,5-tricarboxylic acid (554-95-0) + nickel(II) acetate tetrahydrate (6018-89-9) → [Ni(1,3-bis(4-pyridyl)propane)(H2O)][trimesic acid(2-)] (1174064-14-2)

Guidance literature:

In water; High Pressure; soln. Ni(OAc)2*4H2O and soln. trimesic acid and 1,3-bis(4-pyridyl)propane in cyclohexanol was heated in sealed autoclave at 150°C for 3 days and cooled to room temp. in air; ppt. was filtered, washed with water and dried; elem. anal.;

DOI:10.1002/ejic.200800152

upstream raw materials:

1,3-di(4-pyridyl)propane

benzene-1,3,5-tricarboxylic acid

nickel(II) acetate tetrahydrate