Technology Process of C43H49N5O9
There total 4 articles about C43H49N5O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethylamine / dichloromethane
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine;
In
dichloromethane;
DOI:10.1007/s10989-011-9256-x
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydroxylamine hydrochloride; sodium carbonate / water; tert-butyl alcohol / 1 h / 20 °C
2: chloroamine-T / water; tert-butyl alcohol / 20 °C
3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 5 h / 20 °C
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
5: diethylamine / dichloromethane
6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
With
copper(ll) sulfate pentahydrate; hydroxylamine hydrochloride; chloroamine-T; sodium carbonate; benzotriazol-1-ol; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1007/s10989-011-9256-x
- Guidance literature:
-
Multi-step reaction with 5 steps
1: chloroamine-T / water; tert-butyl alcohol / 20 °C
2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 5 h / 20 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
4: diethylamine / dichloromethane
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
With
copper(ll) sulfate pentahydrate; chloroamine-T; benzotriazol-1-ol; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1007/s10989-011-9256-x