C₂₀H₂₃NO₄

Base Information

Chemical Name:C₂₀H₂₃NO₄
CAS No.:1415723-10-2
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

C<sub>20</sub>H<sub>23</sub>NO<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₀H₂₃NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₃NO₄

Chemical Property:

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Technology Process of C₂₀H₂₃NO₄

There total 5 articles about C₂₀H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1415722-79-0,1415723-35-1
C₂₇H₂₉NO₄

: 1415723-10-2,1421331-72-7
C₂₀H₂₃NO₄

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 17h; under 760.051 Torr; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 57772-57-3
5-hydroxy-2-iodo-benzoic acid

: 1415723-10-2,1421331-72-7
C₂₀H₂₃NO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetone / 5 h / Reflux; Inert atmosphere

2.1: potassium carbonate; copper / Triethylene glycol dimethyl ether / 48 h / 140 °C / Inert atmosphere

2.2: 15 h / 20 - 140 °C / Inert atmosphere

3.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 19 h / 0 - 20 °C / Inert atmosphere

5.1: acetic acid; chromium(VI) oxide / water; acetone / 15 h / 20 °C / Inert atmosphere

6.1: lithium bromide / benzene; cyclohexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

7.1: hydrogen; palladium 10% on activated carbon / methanol / 17 h / 20 °C / 760.05 Torr / Inert atmosphere

With chromium(VI) oxide; palladium 10% on activated carbon; hydrogen; copper; sodium hydride; potassium carbonate; acetic acid; lithium bromide; In tetrahydrofuran; methanol; diethyl ether; Triethylene glycol dimethyl ether; cyclohexane; water; N,N-dimethyl-formamide; acetone; mineral oil; benzene;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 1415684-40-0
C₂₁H₁₇IO₃

: 1415723-10-2,1421331-72-7
C₂₀H₂₃NO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate; copper / Triethylene glycol dimethyl ether / 48 h / 140 °C / Inert atmosphere

1.2: 15 h / 20 - 140 °C / Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

3.2: 19 h / 0 - 20 °C / Inert atmosphere

4.1: acetic acid; chromium(VI) oxide / water; acetone / 15 h / 20 °C / Inert atmosphere

5.1: lithium bromide / benzene; cyclohexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

6.1: hydrogen; palladium 10% on activated carbon / methanol / 17 h / 20 °C / 760.05 Torr / Inert atmosphere

With chromium(VI) oxide; palladium 10% on activated carbon; hydrogen; copper; sodium hydride; potassium carbonate; acetic acid; lithium bromide; In tetrahydrofuran; methanol; diethyl ether; Triethylene glycol dimethyl ether; cyclohexane; water; N,N-dimethyl-formamide; acetone; mineral oil; benzene;
DOI:10.1016/j.tetlet.2012.10.092