Technology Process of C26H40O4
There total 6 articles about C26H40O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-[(trifluoroacetoxy)iodo]benzene;
In
water; acetone;
at 0 ℃;
for 0.5h;
Inert atmosphere;
Darkness;
DOI:10.1021/jo4026868
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine; hydroxylamine hydrochloride / ethanol / 2 h / 20 °C / Inert atmosphere; Large scale
2.1: tert-butylhypochlorite; triethylamine / ethanol; diethyl ether / -78 - 20 °C / Inert atmosphere; Large scale
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Large scale
4.1: samarium diiodide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Large scale
4.2: 0.5 h / 20 °C / Large scale
5.1: bis-[(trifluoroacetoxy)iodo]benzene / water; acetone / 0.5 h / 0 °C / Inert atmosphere; Darkness
With
pyridine; samarium diiodide; tert-butylhypochlorite; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene;
In
tetrahydrofuran; diethyl ether; ethanol; water; acetone;
DOI:10.1021/jo4026868
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Large scale
2.1: samarium diiodide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Large scale
2.2: 0.5 h / 20 °C / Large scale
3.1: bis-[(trifluoroacetoxy)iodo]benzene / water; acetone / 0.5 h / 0 °C / Inert atmosphere; Darkness
With
samarium diiodide; tetrabutyl ammonium fluoride; bis-[(trifluoroacetoxy)iodo]benzene;
In
tetrahydrofuran; water; acetone;
DOI:10.1021/jo4026868