N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide

Base Information

Chemical Name:N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide
CAS No.:1438886-31-7
Molecular Formula:C₂₃H₂₅NO₂S
Molecular Weight:379.523
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide

There total 2 articles about N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 103-67-3
benzyl-methyl-amine

: 98-59-9
p-toluenesulfonyl chloride

: 1438886-29-3
N-(1,2-diphenylpropyl)-N,4-dimethylbenzenesulfonamide

: 1438886-31-7
N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: styrene; benzyl-methyl-amine; With tetrakis(dimethylamido)titanium(IV); 2-(N-methylamino)pyridine; In hexane; at 140 ℃; for 96h; Schlenk technique; Inert atmosphere;

p-toluenesulfonyl chloride; With sodium hydroxide; In water; Overall yield = 69 %; Overall yield = 523 mg; regioselective reaction;
DOI:10.1002/anie.201206027

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 103-67-3
benzyl-methyl-amine

: 98-59-9
p-toluenesulfonyl chloride

: 1438886-31-7
N-(1,3-diphenylpropyl)-N,4-dimethylbenzenesulfonamide

: 3695-02-1
N-benzyl-N-methyl-p-toluenesulfonamide

Guidance literature:: styrene; benzyl-methyl-amine; With bis(dimethylamino)bis(phenyl(6-(phenylamino)pyridine-2-yl)amino)titanium; In hexane; at 140 ℃; for 96h; Inert atmosphere; Schlenk technique; Glovebox;

p-toluenesulfonyl chloride; With sodium hydroxide; In water; for 20h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201403203