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C21H12Br2O

Base Information
  • Chemical Name:C21H12Br2O
  • CAS No.:1395858-24-8
  • Molecular Formula:C21H12Br2O
  • Molecular Weight:440.134
  • Hs Code.:
C<sub>21</sub>H<sub>12</sub>Br<sub>2</sub>O

Synonyms:

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Chemical Property of C21H12Br2O
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Technology Process of C21H12Br2O

There total 1 articles about C21H12Br2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
(3-dibromomethylene-penta-1,4-diynyl)-benzene; With lithium diisopropyl amide; In tetrahydrofuran; hexanes; at -78 ℃; for 1h; Inert atmosphere;
Phenylpropargyl aldehyde; In tetrahydrofuran; hexanes; at -78 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290983
Guidance literature:
With barium manganate; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1055/s-0031-1290983
Guidance literature:
Multi-step reaction with 2 steps
1.1: barium manganate / dichloromethane / 8 h / 20 °C / Inert atmosphere
2.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.2: 0 °C / Inert atmosphere
With barium manganate; triphenylphosphine; In dichloromethane; 2.1: Ramirez dibromoolefination / 2.2: Ramirez dibromoolefination;
DOI:10.1055/s-0031-1290983
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