C₃₀H₄₂O₇Si

Base Information

Chemical Name:C₃₀H₄₂O₇Si
CAS No.:95791-19-8
Molecular Formula:C₃₀H₄₂O₇Si
Molecular Weight:542.745
Hs Code.:

C<sub>30</sub>H<sub>42</sub>O<sub>7</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₄₂O₇Si

Chemical Property:

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Technology Process of C₃₀H₄₂O₇Si

There total 20 articles about C₃₀H₄₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 95791-18-7
C₁₄H₂₄O₇

: 58479-61-1
tert-butylchlorodiphenylsilane

: 95791-19-8
C₃₀H₄₂O₇Si

Guidance literature:: DOI:10.1016/S0040-4039(01)91116-5

Reference yield:

: 82740-87-2
(2R,3S,6R)-2-acetoxymethyl-6-allyl-3,6-dihydro-2H-pyran-3-yl acetate

: 95791-19-8
C₃₀H₄₂O₇Si

Guidance literature:: Multi-step reaction with 19 steps

1: 89 percent / water, trimethylamine / methanol / Ambient temperature

2: 80 percent / d,l-camphorsulfonic acid / CH₂Cl₂ / Ambient temperature

3: 1.) diborane, 2.) 2N NaOH, 30percent H₂O₂ / 1.) THF, -25 deg C, 12 h, 2.) EtOH, RT, overnight

4: pyridine / Ambient temperature

5: MeOH, Dowex 50W (H+) / 9.5 h / Ambient temperature

6: MCPBA / CHCl₃ / 5 °C

7: d,l-camphorsulfonic acid / CHCl₃

8: sodium methoxide / methanol; tetrahydrofuran / 5 °C

9: 1.) DMSO, (COCl)2, 2.) triethylamine / 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, -78 deg C, 10 min.

10: PPTS / CH₂Cl₂ / Ambient temperature

11: 1.) sodium hydride / 1.) DMF, 5 deg C, overnight, 2.) DMF, 70 deg C, 3.5 h

12: 1.) potassium hydride / 1.) DMF, RT, 10 min; 2.) DMF, RT, 30 min.

13: 98 percent / 0.5N HCl / tetrahydrofuran / 3 h / Ambient temperature

14: tetrahydrofuran

15: PCC

16: aluminium- Hg

17: MeOH, acetic acid / 22 h / Heating

18: hydrogen / Pd/C / methanol; acetic acid

19: imidazole

With pyridine; 1H-imidazole; hydrogenchloride; methanol; sodium hydroxide; oxalyl dichloride; aluminium amalgam; Dowex 50W (H+); camphor-10-sulfonic acid; water; hydrogen; dihydrogen peroxide; sodium methylate; pyridinium p-toluenesulfonate; potassium hydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; diborane; trimethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetic acid;
DOI:10.1016/S0040-4020(01)86916-7

Reference yield:

: 95791-07-4
(2R,3S,6R)-6-allyl-2-hydroxymethyl-3,6-dihydro-2H-pyran-3-ol

: 95791-19-8
C₃₀H₄₂O₇Si

Guidance literature:: Multi-step reaction with 18 steps

1: 80 percent / d,l-camphorsulfonic acid / CH₂Cl₂ / Ambient temperature

2: 1.) diborane, 2.) 2N NaOH, 30percent H₂O₂ / 1.) THF, -25 deg C, 12 h, 2.) EtOH, RT, overnight

3: pyridine / Ambient temperature

4: MeOH, Dowex 50W (H+) / 9.5 h / Ambient temperature

5: MCPBA / CHCl₃ / 5 °C

6: d,l-camphorsulfonic acid / CHCl₃

7: sodium methoxide / methanol; tetrahydrofuran / 5 °C

8: 1.) DMSO, (COCl)2, 2.) triethylamine / 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, -78 deg C, 10 min.

9: PPTS / CH₂Cl₂ / Ambient temperature

10: 1.) sodium hydride / 1.) DMF, 5 deg C, overnight, 2.) DMF, 70 deg C, 3.5 h

11: 1.) potassium hydride / 1.) DMF, RT, 10 min; 2.) DMF, RT, 30 min.

12: 98 percent / 0.5N HCl / tetrahydrofuran / 3 h / Ambient temperature

13: tetrahydrofuran

14: PCC

15: aluminium- Hg

16: MeOH, acetic acid / 22 h / Heating

17: hydrogen / Pd/C / methanol; acetic acid

18: imidazole

With pyridine; 1H-imidazole; hydrogenchloride; methanol; sodium hydroxide; oxalyl dichloride; aluminium amalgam; Dowex 50W (H+); camphor-10-sulfonic acid; hydrogen; dihydrogen peroxide; sodium methylate; pyridinium p-toluenesulfonate; potassium hydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; diborane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetic acid;
DOI:10.1016/S0040-4020(01)86916-7