C₂₉H₃₈N₂O₄

Base Information

• Chemical Name: C₂₉H₃₈N₂O₄
• CAS No.: 1404541-20-3
• Molecular Formula: C₂₉H₃₈N₂O₄
• Molecular Weight: 478.632

Synonyms:

Chemical Property of C₂₉H₃₈N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₈N₂O₄

There total 28 articles about C₂₉H₃₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 3-isobutyl-2-piperidine-1-ylcyclobutanecarboxylate (1404378-77-3) → C29H38N2O4 (1404541-20-3) + C29H38N2O4 (1404541-17-8) + C29H38N2O4 (1404541-16-7) + C29H38N2O4 (1404541-23-6)

Guidance literature:

Multi-step reaction with 16 steps

1.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

1.2: 4 h / 95 °C

2.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

4.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

4.2: Cooling with ice

5.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

5.2: 0.33 h / Cooling with ice

6.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane / chloroform

8.1: sodium carbonate / ethanol / 1.5 h / 80 °C

9.1: Iodine monochloride / dichloromethane / 2 h / 0 - 20 °C

10.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 80 °C

11.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.67 h / 0 - 70 °C

12.1: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 1.67 h / 20 °C / Phosphate buffer

13.1: potassium carbonate / N,N-dimethyl-formamide / 1.33 h / 20 °C

14.1: trifluoroacetic acid / chloroform / 2.67 h / 20 - 50 °C

15.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

16.1: hydrogen bromide; acetic acid / water / 1.5 h / 20 - 50 °C

With sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; hydrogen bromide; hydrogen; Iodine monochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium carbonate; potassium carbonate; benzotriazol-1-ol; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; methyl p-toluene sulfonate; triphenylphosphine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; rhodium contaminated with carbon; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

1-(2,2-Dibromovinyl)-3-isobutylcyclobutane (1404378-82-0) → C29H38N2O4 (1404541-20-3) + C29H38N2O4 (1404541-17-8) + C29H38N2O4 (1404541-16-7) + C29H38N2O4 (1404541-23-6)

Guidance literature:

Multi-step reaction with 11 steps

1: n-butyllithium / tetrahydrofuran / -78 - 0 °C

2: sodium hydrogencarbonate; Dess-Martin periodane / chloroform

3: sodium carbonate / ethanol / 1.5 h / 80 °C

4: Iodine monochloride / dichloromethane / 2 h / 0 - 20 °C

5: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 80 °C

6: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.67 h / 0 - 70 °C

7: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 1.67 h / 20 °C / Phosphate buffer

8: potassium carbonate / N,N-dimethyl-formamide / 1.33 h / 20 °C

9: trifluoroacetic acid / chloroform / 2.67 h / 20 - 50 °C

10: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

11: hydrogen bromide; acetic acid / water / 1.5 h / 20 - 50 °C

With sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; hydrogen bromide; Iodine monochloride; sodium hydrogencarbonate; sodium carbonate; potassium carbonate; benzotriazol-1-ol; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

4-Methylpentanoic acid (646-07-1) → C29H38N2O4 (1404541-20-3) + C29H38N2O4 (1404541-17-8) + C29H38N2O4 (1404541-16-7) + C29H38N2O4 (1404541-23-6)

Guidance literature:

Multi-step reaction with 19 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

3.1: hydroquinone / acetonitrile / 95 °C

4.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

4.2: 4 h / 95 °C

5.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

7.2: Cooling with ice

8.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

8.2: 0.33 h / Cooling with ice

9.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C

10.1: sodium hydrogencarbonate; Dess-Martin periodane / chloroform

11.1: sodium carbonate / ethanol / 1.5 h / 80 °C

12.1: Iodine monochloride / dichloromethane / 2 h / 0 - 20 °C

13.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 80 °C

14.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.67 h / 0 - 70 °C

15.1: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 1.67 h / 20 °C / Phosphate buffer

16.1: potassium carbonate / N,N-dimethyl-formamide / 1.33 h / 20 °C

17.1: trifluoroacetic acid / chloroform / 2.67 h / 20 - 50 °C

18.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

19.1: hydrogen bromide; acetic acid / water / 1.5 h / 20 - 50 °C

With sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,1,3,3-Tetramethyldisiloxane; tetrabutyl ammonium fluoride; hydrogen bromide; hydrogen; Iodine monochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium carbonate; potassium carbonate; benzotriazol-1-ol; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;

upstream raw materials:

4-Methylpentanoic acid

4-methyl-1-piperidine-1-ylpentan-1-one

ethyl 3-isobutyl-2-piperidine-1-ylcyclobutanecarboxylate

3-isobutyl-1-cyclobutenecarboxylic acid

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