N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

Base Information

Chemical Name:N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine
CAS No.:120285-32-7
Molecular Formula:C₂₃H₄₁N₃O₅
Molecular Weight:439.596
Hs Code.:

N-<N<sup>α</sup>-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

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Chemical Property of N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

Chemical Property:

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Technology Process of N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

There total 7 articles about N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126333-41-3
N-α-(1-carboxy-3-cyclohexylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>-N-cyclopentyl glycine

: 120285-32-7,126333-56-0,126453-26-7
N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

Guidance literature:: With hydrogen; palladium; In methanol; for 3h; Ambient temperature;

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 120285-32-7,126333-56-0,126453-26-7
N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

Guidance literature:: Multi-step reaction with 5 steps

1: 10.5 g / hydroxybenzotriazole, water-soluble carbodiimide / dimethylformamide / 1 h / 0 °C

2: 9.2 g / 5N NaOH / ethanol; H₂O / 20 h / Ambient temperature

3: trifluoroacetic acid, anisol / 1 h / -20 °C

4: 1.) molecular sieves 3A, Et₃N, 2.) NaBH₃CN, 3.) Dowex 50W-X₂ / 1.) MeOH, room temperature, 30 min, 2.) MeOH, room temperature

5: 250 mg / H₂ / Pd-black / methanol / 3 h / Ambient temperature

With sodium hydroxide; 3 A molecular sieve; DOWEX 50W-X₂; hydrogen; sodium cyanoborohydride; benzotriazol-1-ol; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; palladium; In methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 84126-69-2
N-cyclopentyl glycine ethyl ester hydrochloride

: 120285-32-7,126333-56-0,126453-26-7
N-α-(1-carboxy-3-cyclohexylpropyl)-L-lysyl>-N-cyclopentyl glycine

Guidance literature:: Multi-step reaction with 5 steps

1: 10.5 g / hydroxybenzotriazole, water-soluble carbodiimide / dimethylformamide / 1 h / 0 °C

2: 9.2 g / 5N NaOH / ethanol; H₂O / 20 h / Ambient temperature

3: trifluoroacetic acid, anisol / 1 h / -20 °C

4: 1.) molecular sieves 3A, Et₃N, 2.) NaBH₃CN, 3.) Dowex 50W-X₂ / 1.) MeOH, room temperature, 30 min, 2.) MeOH, room temperature

5: 250 mg / H₂ / Pd-black / methanol / 3 h / Ambient temperature

With sodium hydroxide; 3 A molecular sieve; DOWEX 50W-X₂; hydrogen; sodium cyanoborohydride; benzotriazol-1-ol; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; palladium; In methanol; ethanol; water; N,N-dimethyl-formamide;