Ta(NNCHPh)(S-2,4,6-C₆H₂-i-Pr₃)3(THF)

Base Information

• Chemical Name: Ta(NNCHPh)(S-2,4,6-C₆H₂-i-Pr₃)3(THF)
• CAS No.: 114198-84-4
• Molecular Formula: C₄H₈O*C₇H₆N₂*3C₁₅H₂₃S*Ta
• Molecular Weight: 1077.43
• Mol file: 114198-84-4.mol

Synonyms:

Chemical Property of Ta(NNCHPh)(S-2,4,6-C₆H₂-i-Pr₃)3(THF)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ta(NNCHPh)(S-2,4,6-C₆H₂-i-Pr₃)3(THF)

There total 1 articles about Ta(NNCHPh)(S-2,4,6-C₆H₂-i-Pr₃)3(THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Ta(CH-t-Bu)(S-2,4,6-C6H2-i-Pr3)3(THF) (114198-88-8) + benzaldehyde azine (588-68-1,28867-76-7,65997-87-7,65997-88-8) → Ta(NNCHPh)(S-2,4,6-C6H2-i-Pr3)3(THF) (114198-84-4)

Guidance literature:

In diethyl ether; byproducts: PhCH=CHCMe3; A soln. of benzaldehyde azine in ether was added to a soln. of Ta(CH-t-Bu)(S-2,4,6-C6H2-i-Pr) in ether at 25°C. The soln. was stirred for 2 h, during which time the color changed from orange to orange-red.; The solvent was removed in vac., and the resulting oil crystallized from pentane at -30°C to yield crystals.;

upstream raw materials:

Ta(CH-t-Bu)(S-2,4,6-C₆H₂-i-Pr₃)3(THF)

benzaldehyde azine