Technology Process of C26H32N2O6
There total 9 articles about C26H32N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane
2: lithium diisopropyl amide
3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water
4: diphenyl phosphoryl azide; triethylamine / toluene
5: palladium on activated charcoal; hydrogen / methanol
6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
With
diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene;
2: Evan's asymmetric alkylation / 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water
2: diphenyl phosphoryl azide; triethylamine / toluene
3: palladium on activated charcoal; hydrogen / methanol
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
With
diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene;
2: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diphenyl phosphoryl azide; triethylamine / toluene
2: palladium on activated charcoal; hydrogen / methanol
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane
With
diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
methanol; dichloromethane; toluene;
1: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014