(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Base Information

Chemical Name:(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate
CAS No.:944479-67-8
Molecular Formula:C₄₂H₅₆F₁₇N₅O₅
Molecular Weight:1033.91
Hs Code.:

(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Synonyms:

Suppliers and Price of (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

There total 7 articles about (2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944479-30-5
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-azido-2,5-dimethylhexanoate

: 944479-67-8
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

2: 100 percent / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

3: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

4: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

5: 66 mg / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

6: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

With dmap; In tetrahydrofuran; dichloromethane; water; 1: Staudinger reaction / 4: Staudinger reaction;
DOI:10.1016/j.tet.2007.03.034

Reference yield:

: C₄₄H₄₁F₁₇NO₃P

: 944479-67-8
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

2: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

3: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

4: 66 mg / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

5: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

With dmap; In tetrahydrofuran; dichloromethane; water; 3: Staudinger reaction;
DOI:10.1016/j.tet.2007.03.034

Reference yield:

: C₂₆H₂₈F₁₇NO₃

: 944479-67-8
(2S,3S)-4-[3-(perfluorooctyl)propyl-1-oxy]benzyl 3-((2S,3S)-3-((2S,3S)-3-azido-2,5-dimethylhexanamido)-2,5-dimethylhexanamido)-2,5-dimethylhexanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

2: tetrahydrofuran / 0.08 h / 120 °C / microwave irradiation

3: 66 mg / tetrahydrofuran; H₂O / 0.17 h / 120 °C / microwave irradiation

4: 4-(dimethylamino)pyridine; 1-ethyl-3-(3'-dimethylaminopropyl) carbodiimide / CH₂Cl₂ / 0.5 h

With dmap; In tetrahydrofuran; dichloromethane; water; 2: Staudinger reaction;
DOI:10.1016/j.tet.2007.03.034