(Et₂PhP)3(H)2IrSi(Cl)CH₂C₆H₂Me₂C₆H₃-mesityl

Base Information

• Chemical Name: (Et₂PhP)3(H)2IrSi(Cl)CH₂C₆H₂Me₂C₆H₃-mesityl
• CAS No.: 610269-76-6
• Molecular Formula: C₅₄H₇₁ClIrP₃Si
• Molecular Weight: 1068.84
• Mol file: 610269-76-6.mol

Synonyms:

Chemical Property of (Et₂PhP)3(H)2IrSi(Cl)CH₂C₆H₂Me₂C₆H₃-mesityl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (Et₂PhP)3(H)2IrSi(Cl)CH₂C₆H₂Me₂C₆H₃-mesityl

There total 1 articles about (Et₂PhP)3(H)2IrSi(Cl)CH₂C₆H₂Me₂C₆H₃-mesityl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

H3Si(C6H3-2,6-(C6H2-2,4,6-Me3)2) (220493-88-9) + (Et2PhP)3(Cl)Ir (610269-75-5) → (Et2PhP)3(H)2IrSi(Cl)CH2C6H2Me2C6H3-mesityl (610269-76-6)

Guidance literature:

In tetrahydrofuran; under N2 or Ar; THF soln. of (Et2PhP)3(Cl)Ir added to H3Si(C6H3-Mes2-2,6) in THF while stirring at dry ice-acetone bath temp.; soln. warmed to ambient temp. and stirred for addnl. 16 h; volatiles removed under reduced pressure; solid washed with hexane and collected on glass frit; elem. anal.;

DOI:10.1016/S0022-328X(03)00629-6

upstream raw materials:

H₃Si(C₆H₃-2,6-(C₆H₂-2,4,6-Me₃)2)

(Et₂PhP)3(Cl)Ir