C₂₄H₂₂N₆O₂S

Base Information

• Chemical Name: C₂₄H₂₂N₆O₂S
• CAS No.: 1384101-63-6
• Molecular Formula: C₂₄H₂₂N₆O₂S
• Molecular Weight: 458.544
• Mol file: 1384101-63-6.mol

Synonyms:

Chemical Property of C₂₄H₂₂N₆O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₂N₆O₂S

There total 5 articles about C₂₄H₂₂N₆O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C18H17N5O3S (1384101-93-2) + aniline (62-53-3) → C24H22N6O2S (1384101-63-6)

Guidance literature:

C₁₈H₁₇N₅O₃S; With 1,1'-carbonyldiimidazole; In tetrahydrofuran;

aniline; In tetrahydrofuran;

DOI:10.1016/j.bmc.2012.04.055

Reference yield:

4-methoxycarbonyl aniline (619-45-4) → C24H22N6O2S (1384101-63-6)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 1,4-dioxane / 8 h / Reflux

2.1: tetrahydrofuran / 20 °C

3.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; butan-1-ol / 48 h / 20 °C

4.1: lithium hydroxide / 1,4-dioxane; water / 20 °C

4.2: pH Ca_. 3 / Cooling with ice

5.1: 1,1'-carbonyldiimidazole / tetrahydrofuran

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; 1,1'-carbonyldiimidazole; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; water; butan-1-ol;

DOI:10.1016/j.bmc.2012.04.055

Reference yield:

C19H19N5O3S (1384101-88-5) → C24H22N6O2S (1384101-63-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium hydroxide / 1,4-dioxane; water / 20 °C

1.2: pH Ca_. 3 / Cooling with ice

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran

With 1,1'-carbonyldiimidazole; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; water;

DOI:10.1016/j.bmc.2012.04.055

upstream raw materials:

C₁₉H₁₉N₅O₃S

C₁₈H₁₇N₅O₃S

aniline

C₁₂H₁₂N₂O₃