C₂₇H₁₉FN₂O₃

Base Information

Chemical Name:C₂₇H₁₉FN₂O₃
CAS No.:1395923-57-5
Molecular Formula:C₂₇H₁₉FN₂O₃
Molecular Weight:438.458
Hs Code.:

C<sub>27</sub>H<sub>19</sub>FN<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₁₉FN₂O₃

Chemical Property:

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Technology Process of C₂₇H₁₉FN₂O₃

There total 6 articles about C₂₇H₁₉FN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 263400-66-4
N-(5-amino-2-fluoro-phenyl)-benzamide

: 60086-50-2
3-Chloro-6,11-dihydrodibenzoxepin-11-one

: 1395923-57-5
C₂₇H₁₉FN₂O₃

Guidance literature:: With palladium diacetate; caesium carbonate; XPhos; In 1,4-dioxane; tert-butyl alcohol; at 110 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jm300951u

Reference yield:

: methyl 2-[(3-chlorophenoxy)methyl]benzoate

: 1395923-57-5
C₂₇H₁₉FN₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / methanol; water / 4 h / Reflux

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3: aluminum (III) chloride / dichloromethane / 0.5 h / 20 °C

4: caesium carbonate; palladium diacetate; XPhos / tert-butyl alcohol; 1,4-dioxane / 3 h / 110 °C / Inert atmosphere

With aluminum (III) chloride; oxalyl dichloride; palladium diacetate; caesium carbonate; N,N-dimethyl-formamide; potassium hydroxide; XPhos; In 1,4-dioxane; methanol; dichloromethane; water; tert-butyl alcohol; 3: |Friedel-Crafts Acylation / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm300951u

Reference yield:

: 2417-73-4
methyl 2-bromomethylbenzoate

: 1395923-57-5
C₂₇H₁₉FN₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: acetone / 6 h / 50 - 70 °C

2: potassium hydroxide / methanol; water / 4 h / Reflux

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4: aluminum (III) chloride / dichloromethane / 0.5 h / 20 °C

5: caesium carbonate; palladium diacetate; XPhos / tert-butyl alcohol; 1,4-dioxane / 3 h / 110 °C / Inert atmosphere

With aluminum (III) chloride; oxalyl dichloride; palladium diacetate; caesium carbonate; N,N-dimethyl-formamide; potassium hydroxide; XPhos; In 1,4-dioxane; methanol; dichloromethane; water; acetone; tert-butyl alcohol; 4: |Friedel-Crafts Acylation / 5: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm300951u