(Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2

Base Information

Chemical Name:(Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2
CAS No.:85717-51-7
Molecular Formula:C₃₈H₂₉ClN₆Ru*2F₆P
Molecular Weight:996.14
Hs Code.:

(Ru(trpy)(bpy)(4'-Cl-stilb))(PF<sub>6</sub>)2

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Chemical Property of (Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2

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Technology Process of (Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2

There total 1 articles about (Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: ammonium hexafluorophosphate

: 16455-13-3
(Ru(trpy)(bpy)Cl)(ClO₄)

: 2502-99-0,5847-63-2,46459-15-8,102045-66-9
(E)-4-(4-chlorostyryl)pyridine

: 85717-51-7
(Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2

Guidance literature:: In ethanol; water; to soln. containing water, ethanol and 4-fold excess 4'-Cl-stilb added (Ru(trpy)(bpy)Cl)ClO4 and mixt. refluxed for 5 h, solvent volume reducedby rotary evapn., saturated aq. soln. NH4PF6 added; soln. cooled, ppt. collected and chromed. with 2:1 toluene/CH3CN as eluant and repptd. from acetone by addn. to ether;

Reference yield:

: 85717-51-7
(Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2

: 85649-78-1
(Ru(trpy)(bpy)(4'-Cl-stilb))(PF₆)2(polymer)

Guidance literature:: In acetonitrile; Electrochem. Process; electropolymerization complex in CH3CN-saturated nitrogen soln. by scanning Pt-disk potential repeatedly ca. 150 mV past E1/2 for the reductionwave of interest;