C₃₀H₂₉F₃N₆O₂

Base Information

Chemical Name:C₃₀H₂₉F₃N₆O₂
CAS No.:1421685-09-7
Molecular Formula:C₃₀H₂₉F₃N₆O₂
Molecular Weight:562.594
Hs Code.:

C<sub>30</sub>H<sub>29</sub>F<sub>3</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₃₀H₂₉F₃N₆O₂

Chemical Property:

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Technology Process of C₃₀H₂₉F₃N₆O₂

There total 9 articles about C₃₀H₂₉F₃N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1086064-44-9
5-bromo-1H-pyrazolo[3,4-b]pyridin-3-ol

: 1421685-09-7
C₃₀H₂₉F₃N₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / dimethyl sulfoxide / 1 h / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 0.25 h

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 80 °C / Sealed tube; Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; sodium hydride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide; 3: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301581y

Reference yield:

: 90347-66-3
methyl 3-iodo-4-methylbenzoate

: 1421685-09-7
C₃₀H₂₉F₃N₆O₂

Guidance literature:: Multi-step reaction with 5 steps

1: potassium tert-butylate / tetrahydrofuran / 3 h / -20 - 20 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 - 60 °C / Inert atmosphere

3: potassium carbonate; methanol / 20 °C / Inert atmosphere

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 80 °C / Sealed tube; Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / Reflux

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile; 2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301581y

Reference yield:

: 1186608-87-6
5-bromo-1-[(4-methoxyphenyl)methyl]pyrazolo[3,4-b]pyridin-3-ol

: 1421685-09-7
C₃₀H₂₉F₃N₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 0.25 h

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 80 °C / Sealed tube; Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Sonogashira Cross-Coupling;
DOI:10.1021/jm301581y