Technology Process of 2-methoxy-5-(5,6,7-trimethoxyindol-1-yl)phenol
There total 6 articles about 2-methoxy-5-(5,6,7-trimethoxyindol-1-yl)phenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; copper(II) oxide;
In
N,N-dimethyl-formamide;
at 160 ℃;
for 0.166667h;
Microwave irradiation;
DOI:10.1039/c0ob01038c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: boron trifluoride-tetrahydrofuran complex / tetrahydrofuran / Reflux
2: dipyridinium dichromate / dichloromethane / 20 h / Molecular sieve
3: ammonium acetate / acetic acid / 1.5 h / 100 °C
4: iron / ethanol; acetic acid / 2 h / 100 °C
5: potassium carbonate; copper(II) oxide / N,N-dimethyl-formamide / 0.17 h / 160 °C / Microwave irradiation
With
dipyridinium dichromate; boron trifluoride-tetrahydrofuran complex; ammonium acetate; iron; potassium carbonate; copper(II) oxide;
In
tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01038c
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium hydroxide / methanol / 1 h / Reflux
2: boron trifluoride-tetrahydrofuran complex / tetrahydrofuran / Reflux
3: dipyridinium dichromate / dichloromethane / 20 h / Molecular sieve
4: ammonium acetate / acetic acid / 1.5 h / 100 °C
5: iron / ethanol; acetic acid / 2 h / 100 °C
6: potassium carbonate; copper(II) oxide / N,N-dimethyl-formamide / 0.17 h / 160 °C / Microwave irradiation
With
dipyridinium dichromate; boron trifluoride-tetrahydrofuran complex; ammonium acetate; iron; potassium carbonate; copper(II) oxide; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01038c
