OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)

Base Information

Chemical Name:OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)
CAS No.:1272970-99-6
Molecular Formula:C₂₉H₅₈N₂OOsP₂
Molecular Weight:702.94
Hs Code.:

OsH<sub>4</sub>(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)

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Technology Process of OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)

There total 1 articles about OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 24155-47-3,27656-18-4
1-phenyl-2-(1-imidazolyl)ethanol

: 131296-74-7
Os(hydride)6(triisopropylphosphine)2

: 1272970-99-6
OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)

Guidance literature:: In tetrahydrofuran; byproducts: H2; under rigorous exclusion of air using Schlenk techniques; soln. of Os complex in THF was treated with 1.2 equiv. of ligand; soln. heated under reflux for 17 h; cooled to room temp.; filtered; solvent removed; MeOH added to the residue at 223 K; solid washed (MeOH); dried (vac.); elem. anal.;
DOI:10.1021/om101173e

Reference yield: 33.0%

: 1272970-99-6
OsH₄(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazole)

: [OsH₃(P(iso-propyl)3)2(1-(2-hydroxy-2-phenylethyl)imidazolium(-2H))]

Guidance literature:: In toluene; byproducts: H2; under rigorous exclusion of air using Schlenk techniques; soln. of Os complex in toluene was heated under reflux for 17 h; cooled to room temp.; filtered; solvent removed; pentane added to the residue at 223 K; solid washed (pentane); dried (vac.); elem. anal.;
DOI:10.1021/om101173e