C₂₅H₃₅NO₄Si

Base Information

Chemical Name:C₂₅H₃₅NO₄Si
CAS No.:1591632-91-5
Molecular Formula:C₂₅H₃₅NO₄Si
Molecular Weight:441.643
Hs Code.:

C<sub>25</sub>H<sub>35</sub>NO<sub>4</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₅NO₄Si

Chemical Property:

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Technology Process of C₂₅H₃₅NO₄Si

There total 11 articles about C₂₅H₃₅NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 941-69-5
N-phenyl-maleimide

: 1591633-09-8
3-tert-butyldimethylsilyloxy-5-ethenyl-3-methylcyclohex-5-en-1-ol

: 1591632-91-5
C₂₅H₃₅NO₄Si

Guidance literature:: at 20 ℃; for 30h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201301627

Reference yield:

: 169310-73-0
1-methoxy-4-((3-methylbut-3-en-1-yl)oxy)benzene

: 1591632-91-5
C₂₅H₃₅NO₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: AD-mix-α; water; methanesulfonamide / tert-butyl alcohol / 14 h / 0 °C

2.1: pyridine / 3 h / 0 °C

3.1: dimethyl sulfoxide / 16 h / Inert atmosphere

4.1: collidine / dichloromethane / 12 h / 0 °C

5.1: ammonium cerium (IV) nitrate / acetonitrile; water / 0.08 h / 0 °C

6.1: Dess-Martin periodane / dichloromethane / 8 h / 20 °C / Inert atmosphere

7.1: tetrahydrofuran; toluene / 2 h / -78 - 20 °C / Inert atmosphere

8.1: Grubbs catalyst first generation / dichloromethane / 24 h / Inert atmosphere

8.2: 16 h

9.1: 30 h / 320 °C / Inert atmosphere

10.1: silica gel / Petroleum ether; ethyl acetate

With pyridine; Grubbs catalyst first generation; ammonium cerium (IV) nitrate; methanesulfonamide; AD-mix-α; water; silica gel; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; toluene; acetonitrile; Petroleum ether; tert-butyl alcohol; 1.1: |Sharpless Dihydroxylation / 6.1: |Dess-Martin Oxidation / 9.1: |Diels-Alder Cycloaddition;
DOI:10.1002/ejoc.201301627

Reference yield:

: 763-32-6
2-methyl-1-buten-4-ol

: 1591632-91-5
C₂₅H₃₅NO₄Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12 h / 0 - 20 °C

2.1: AD-mix-α; water; methanesulfonamide / tert-butyl alcohol / 14 h / 0 °C

3.1: pyridine / 3 h / 0 °C

4.1: dimethyl sulfoxide / 16 h / Inert atmosphere

5.1: collidine / dichloromethane / 12 h / 0 °C

6.1: ammonium cerium (IV) nitrate / acetonitrile; water / 0.08 h / 0 °C

7.1: Dess-Martin periodane / dichloromethane / 8 h / 20 °C / Inert atmosphere

8.1: tetrahydrofuran; toluene / 2 h / -78 - 20 °C / Inert atmosphere

9.1: Grubbs catalyst first generation / dichloromethane / 24 h / Inert atmosphere

9.2: 16 h

10.1: 30 h / 320 °C / Inert atmosphere

11.1: silica gel / Petroleum ether; ethyl acetate

With pyridine; Grubbs catalyst first generation; ammonium cerium (IV) nitrate; methanesulfonamide; AD-mix-α; di-isopropyl azodicarboxylate; water; silica gel; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; toluene; acetonitrile; Petroleum ether; tert-butyl alcohol; 2.1: |Sharpless Dihydroxylation / 7.1: |Dess-Martin Oxidation / 10.1: |Diels-Alder Cycloaddition;
DOI:10.1002/ejoc.201301627