C₁₄H₂₂O₄

Base Information

Chemical Name:C₁₄H₂₂O₄
CAS No.:1622095-28-6
Molecular Formula:C₁₄H₂₂O₄
Molecular Weight:254.326
Hs Code.:

C<sub>14</sub>H<sub>22</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₂O₄

Chemical Property:

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Technology Process of C₁₄H₂₂O₄

There total 10 articles about C₁₄H₂₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 166376-61-0
C₁₄H₂₀O₃

: 1622095-28-6
C₁₄H₂₂O₄

Guidance literature:: C₁₄H₂₀O₃; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 9h; Inert atmosphere; Cooling with ice;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejoc.201402096

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1622095-28-6
C₁₄H₂₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2.1: sodium hydroxide; water

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 14 h / 20 °C

4.1: dichloromethane / 20 h / 20 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

5.2: 11.5 h / -78 - -5 °C

6.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

8.1: dimethylsulfide borane complex / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere; Cooling with ice

8.2: 5 h / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; dimethylsulfide borane complex; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; 4.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622095-12-8
C₂₀H₁₉NO₅

: 1622095-28-6
C₁₄H₂₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 20 h / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

2.2: 11.5 h / -78 - -5 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

4.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

5.1: dimethylsulfide borane complex / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere; Cooling with ice

5.2: 5 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; dimethylsulfide borane complex; sodium hexamethyldisilazane; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; cyclohexane; water; 1.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096