Technology Process of C71H78Cl3NO21
There total 6 articles about C71H78Cl3NO21 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / EtN(i-Pr)2
2: 92 percent / BF3*Et2O / CH2Cl2
3: 93 percent / DMP, EtN(iPr)2 / CH2Cl2 / 72 h / Ambient temperature
4: 1.) NIS, 2.) TMSOTf / 1.) CH2Cl2, 1 h, 2.) -30 deg C, 30 min
With
N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; phthalic acid dimethyl ester; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1016/S0008-6215(96)00237-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: NaHCO3 / H2O / 1 h
2: pyridine / Ambient temperature
3: 92 percent / BF3*Et2O / CH2Cl2
4: 93 percent / DMP, EtN(iPr)2 / CH2Cl2 / 72 h / Ambient temperature
5: 1.) NIS, 2.) TMSOTf / 1.) CH2Cl2, 1 h, 2.) -30 deg C, 30 min
With
pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; phthalic acid dimethyl ester; boron trifluoride diethyl etherate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; water;
DOI:10.1016/S0008-6215(96)00237-6
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / Ambient temperature
2: 92 percent / BF3*Et2O / CH2Cl2
3: 93 percent / DMP, EtN(iPr)2 / CH2Cl2 / 72 h / Ambient temperature
4: 1.) NIS, 2.) TMSOTf / 1.) CH2Cl2, 1 h, 2.) -30 deg C, 30 min
With
pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; phthalic acid dimethyl ester; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1016/S0008-6215(96)00237-6
