Technology Process of C14H10FN5S
There total 3 articles about C14H10FN5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
aq. phosphate buffer; acetonitrile;
at 30 ℃;
pH=7.0;
DOI:10.1021/jo400826f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 5%-palladium/activated carbon; hydrazine hydrate / tetrahydrofuran / -30 - 20 °C / Inert atmosphere
2: N-ethylmorpholine; / acetonitrile / 1.5 h / -10 - 0 °C / Inert atmosphere
3: sodium azide / aq. phosphate buffer; acetonitrile / 30 °C / pH 7.0
With
N-ethylmorpholine;; sodium azide; 5%-palladium/activated carbon; hydrazine hydrate;
In
tetrahydrofuran; aq. phosphate buffer; acetonitrile;
DOI:10.1021/jo400826f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethylmorpholine; / acetonitrile / 1.5 h / -10 - 0 °C / Inert atmosphere
2: sodium azide / aq. phosphate buffer; acetonitrile / 30 °C / pH 7.0
With
N-ethylmorpholine;; sodium azide;
In
aq. phosphate buffer; acetonitrile;
DOI:10.1021/jo400826f