C₂₄H₂₉NO₅

Base Information

Chemical Name:C₂₄H₂₉NO₅
CAS No.:1579996-47-6
Molecular Formula:C₂₄H₂₉NO₅
Molecular Weight:411.498
Hs Code.:

C<sub>24</sub>H<sub>29</sub>NO<sub>5</sub>

Synonyms:

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Chemical Property of C₂₄H₂₉NO₅

Chemical Property:

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Technology Process of C₂₄H₂₉NO₅

There total 9 articles about C₂₄H₂₉NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1579996-45-4
tert-butyl (2S,3R,4R)-3,4-bis(benzyloxy)-2-(hydroxymethyl)pyrrolidine-1-carboxylate

: 1579996-47-6
C₂₄H₂₉NO₅

Guidance literature:: With pyridine; chromium(VI) oxide; acetic anhydride; In dichloromethane; at 0 - 20 ℃; for 1.25h; Inert atmosphere;
DOI:10.1039/c3ra47555g

Reference yield:

: (4R,5R,6R)-4,5-bis(benzyloxy)-6-(trityloxymethyl)tetrahydro-2H-pyran-2,3-diol

: 1579996-47-6
C₂₄H₂₉NO₅

Guidance literature:: Multi-step reaction with 8 steps

1: sodium periodate; sodium hydrogencarbonate / water; ethanol / 4 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1.08 h / 0 - 20 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

4: 2 h / 70 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

7: sodium carbonate / ethyl acetate / 2 h / 20 °C / Inert atmosphere

8: chromium(VI) oxide; acetic anhydride; pyridine / dichloromethane / 1.25 h / 0 - 20 °C / Inert atmosphere

With pyridine; chromium(VI) oxide; dmap; sodium tetrahydroborate; sodium periodate; 10 wt% Pd(OH)2 on carbon; hydrogen; acetic anhydride; sodium hydrogencarbonate; sodium carbonate; triethylamine; trifluoroacetic acid; In methanol; ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1039/c3ra47555g

Reference yield:

: 155931-85-4
(2R,3R,4S)-3,4-bis(benzyloxy)-5-oxo-1-(trityloxy)pentan-2-yl formate

: 1579996-47-6
C₂₄H₂₉NO₅

Guidance literature:: Multi-step reaction with 7 steps

1: sodium tetrahydroborate / methanol / 1.08 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

3: 2 h / 70 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

6: sodium carbonate / ethyl acetate / 2 h / 20 °C / Inert atmosphere

7: chromium(VI) oxide; acetic anhydride; pyridine / dichloromethane / 1.25 h / 0 - 20 °C / Inert atmosphere

With pyridine; chromium(VI) oxide; dmap; sodium tetrahydroborate; 10 wt% Pd(OH)2 on carbon; hydrogen; acetic anhydride; sodium carbonate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c3ra47555g