Technology Process of C37H38NO2PS
There total 3 articles about C37H38NO2PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine;
In
dichloromethane;
at 20 ℃;
for 3h;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c3nj01308a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C / Schlenk technique; Inert atmosphere
1.2: 3 h / 20 °C / Schlenk technique; Inert atmosphere
2.1: sodium hydride; 18-crown-6 ether / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Schlenk technique; Inert atmosphere
3.1: iodine / dichloromethane / 3 h / 20 °C / Schlenk technique; Inert atmosphere
With
18-crown-6 ether; iodine; sodium hydride;
In
tetrahydrofuran; dichloromethane; mineral oil;
2.1: |Wittig Olefination;
DOI:10.1039/c3nj01308a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride; 18-crown-6 ether / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Schlenk technique; Inert atmosphere
2: iodine / dichloromethane / 3 h / 20 °C / Schlenk technique; Inert atmosphere
With
18-crown-6 ether; iodine; sodium hydride;
In
tetrahydrofuran; dichloromethane; mineral oil;
1: |Wittig Olefination;
DOI:10.1039/c3nj01308a
