N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide

Base Information

• Chemical Name: N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide
• CAS No.: 114643-67-3
• Molecular Formula: C₂₉H₄₂N₂O₁₅
• Molecular Weight: 658.657

Synonyms:

Chemical Property of N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide

Chemical Property:

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Useful:

Technology Process of N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide

There total 1 articles about N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl bromide (89950-89-0) + 2-Acetamido-1,6-anhydro-3-O-benzyl-2-desoxy-β-D-glucopyranose (50604-73-4) → N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide (114643-67-3)

Guidance literature:

With mercury(II) cyanide; In nitromethane; benzene; Ambient temperature;

DOI:10.1016/0008-6215(87)80251-3

Reference yield:

acetic anhydride (108-24-7) + N-{(1R,2S,3R,4R,5R)-2-[(2S,3R,4S,5S,6R)-4-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-3-benzyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl}-acetamide (114643-67-3) → O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-β-D-glucopyranoside (114643-68-4)

Guidance literature:

In pyridine; Yield given; Ambient temperature;

DOI:10.1016/0008-6215(87)80251-3

upstream raw materials:

3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl bromide

2-Acetamido-1,6-anhydro-3-O-benzyl-2-desoxy-β-D-glucopyranose

Downstream raw materials:

O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-1,6-anhydro-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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