C₂₄H₂₄BrN₃O₅

Base Information

Chemical Name:C₂₄H₂₄BrN₃O₅
CAS No.:1609689-74-8
Molecular Formula:C₂₄H₂₄BrN₃O₅
Molecular Weight:514.376
Hs Code.:

C<sub>24</sub>H<sub>24</sub>BrN<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₄H₂₄BrN₃O₅

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Technology Process of C₂₄H₂₄BrN₃O₅

There total 2 articles about C₂₄H₂₄BrN₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2577-48-2
methyl (2S)-pyrrolidine carboxylate

: 1609689-74-8
C₂₄H₂₄BrN₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-Nitrophenyl chloroformate; pyridine / dichloromethane / 18 h

1.2: 3 h / Reflux

2.1: lithium hydroxide; water / methanol; tetrahydrofuran

2.2: 18 h

2.3: 3 h

With pyridine; water; 4-Nitrophenyl chloroformate; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.04.002

Reference yield:

: 199118-68-8
H-Asp(OBzl)-CONH₂ hydrochloride

: 1609689-72-6
C₁₄H₁₆BrNO₄

: 1609689-74-8
C₂₄H₂₄BrN₃O₅

Guidance literature:: C₁₄H₁₆BrNO₄; With water; lithium hydroxide; In tetrahydrofuran; methanol;

H-Asp(OBzl)-CONH₂ hydrochloride; With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; for 18h;

With 1,3,5-trichloro-2,4,6-triazine; In N,N-dimethyl-formamide; for 3h;
DOI:10.1016/j.bmcl.2014.04.002

Reference yield:

: 1609689-74-8
C₂₄H₂₄BrN₃O₅

: 1609689-80-6
C₂₃H₂₄N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide; water / tetrahydrofuran

1.2: 18 h

2.1: sodium carbonate / N,N-dimethyl-formamide; water / 60 °C

With water; sodium carbonate; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.04.002