N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide
CAS No.:1616405-59-4
Molecular Formula:C₂₃H₂₂N₂O₂S
Molecular Weight:390.506
Hs Code.:

Synonyms:

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Chemical Property of N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide

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Technology Process of N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide

There total 6 articles about N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 620-05-3
iodomethylbenzene

: 1616405-59-4
N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

2: copper(I) thiophene-2-carboxylate / toluene / 2 h / 20 °C / Inert atmosphere

3: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / 60 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / 14 h / 20 °C / 2327.23 Torr / Inert atmosphere

With copper(I) thiophene-2-carboxylate; rhodium (II) octanoate dimer; palladium 10% on activated carbon; hydrogen; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol501618z

Reference yield:

: 1616405-47-0
N-benzyl-N-((1-tosyl-1H-1,2,3-triazol-4-yl)methyl)aniline

: 1616405-59-4
N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / 60 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / 14 h / 20 °C / 2327.23 Torr / Inert atmosphere

With rhodium (II) octanoate dimer; palladium 10% on activated carbon; hydrogen; In 1,2-dichloro-ethane;
DOI:10.1021/ol501618z

Reference yield:

: 14465-74-8
N-phenyl-N-prop-2-ynylamine

: 1616405-59-4
N-((1-benzyl-1H-indol-3-yl)methyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

2: copper(I) thiophene-2-carboxylate / toluene / 2 h / 20 °C / Inert atmosphere

3: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / 60 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / 14 h / 20 °C / 2327.23 Torr / Inert atmosphere

With copper(I) thiophene-2-carboxylate; rhodium (II) octanoate dimer; palladium 10% on activated carbon; hydrogen; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol501618z