Technology Process of C62H95N9O12
There total 5 articles about C62H95N9O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C47H78N6O10;
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.333333h;
Inert atmosphere;
N-(2-amino-ethyl)-2-(7-dimethylamino-2-oxo-2H-chromen-4-yl)-acetamide;
In
dichloromethane;
at 20 ℃;
for 12h;
DOI:10.1021/np300834q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere
2.1: lithium hydroxide / tetrahydrofuran; tert-butyl alcohol; water / 20 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 0.33 h / Inert atmosphere
3.2: 12 h / 20 °C
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/np300834q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide / tetrahydrofuran; tert-butyl alcohol; water / 20 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 0.33 h / Inert atmosphere
2.2: 12 h / 20 °C
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/np300834q
