C₄₁H₃₇O₁₁P

Base Information

Chemical Name:C₄₁H₃₇O₁₁P
CAS No.:1375486-79-5
Molecular Formula:C₄₁H₃₇O₁₁P
Molecular Weight:736.712
Hs Code.:

C<sub>41</sub>H<sub>37</sub>O<sub>11</sub>P

Synonyms:

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Chemical Property of C₄₁H₃₇O₁₁P

Chemical Property:

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Technology Process of C₄₁H₃₇O₁₁P

There total 9 articles about C₄₁H₃₇O₁₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20869-13-0
methyl 5,6-O-isopropylidine-α-D-galactofuranoside

: 1375486-79-5
C₄₁H₃₇O₁₁P

Guidance literature:: Multi-step reaction with 8 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.1: sodium phenyl-methanolate / 12 h / 90 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere

3.2: 3 h / Inert atmosphere

3.3: Inert atmosphere

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 50 - 110 °C / Inert atmosphere

5.1: hydrogenchloride / methanol; dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / 12 h / 20 °C / 760.05 Torr / Inert atmosphere

7.1: pyridine / 12 h / 0 - 20 °C / Inert atmosphere

8.1: hydrogen bromide; acetic acid / dichloromethane / Inert atmosphere

8.2: Inert atmosphere

With pyridine; hydrogenchloride; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen bromide; hydrogen; tri-n-butyl-tin hydride; sodium hydride; acetic acid; sodium phenyl-methanolate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil; 1.1: Mitsunobu reaction;
DOI:10.1039/c2ob25159k

Reference yield:

: C₇H₁₄O₆

: 1375486-79-5
C₄₁H₃₇O₁₁P

Guidance literature:: Multi-step reaction with 9 steps

1.1: camphor-10-sulfonic acid; 2,2-dimethoxy-propane / 2 h / 20 °C / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: sodium phenyl-methanolate / 12 h / 90 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere

4.2: 3 h / Inert atmosphere

4.3: Inert atmosphere

5.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 50 - 110 °C / Inert atmosphere

6.1: hydrogenchloride / methanol; dichloromethane / 1 h / 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / 12 h / 20 °C / 760.05 Torr / Inert atmosphere

8.1: pyridine / 12 h / 0 - 20 °C / Inert atmosphere

9.1: hydrogen bromide; acetic acid / dichloromethane / Inert atmosphere

9.2: Inert atmosphere

With pyridine; hydrogenchloride; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen bromide; hydrogen; tri-n-butyl-tin hydride; sodium hydride; acetic acid; sodium phenyl-methanolate; triphenylphosphine; 2,2-dimethoxy-propane; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil; 2.1: Mitsunobu reaction;
DOI:10.1039/c2ob25159k

Reference yield:

: 1375486-72-8
methyl 2,3-anhydro-5,6-O-isopropylidine-β-D-galactofuranoside

: 1375486-79-5
C₄₁H₃₇O₁₁P

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium phenyl-methanolate / 12 h / 90 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere

2.3: Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 50 - 110 °C / Inert atmosphere

4.1: hydrogenchloride / methanol; dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / 12 h / 20 °C / 760.05 Torr / Inert atmosphere

6.1: pyridine / 12 h / 0 - 20 °C / Inert atmosphere

7.1: hydrogen bromide; acetic acid / dichloromethane / Inert atmosphere

7.2: Inert atmosphere

With pyridine; hydrogenchloride; 2,2'-azobis(isobutyronitrile); palladium 10% on activated carbon; hydrogen bromide; hydrogen; tri-n-butyl-tin hydride; sodium hydride; acetic acid; sodium phenyl-methanolate; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
DOI:10.1039/c2ob25159k