trans-dichlorobis(2,2'-bipyridyl-4,4'-dicarboxylic acid)ruthenium(II)

Base Information

Chemical Name:trans-dichlorobis(2,2'-bipyridyl-4,4'-dicarboxylic acid)ruthenium(II)
CAS No.:123049-50-3
Molecular Formula:C₂₄H₁₆Cl₂N₄O₈Ru
Molecular Weight:660.389
Hs Code.:

Synonyms:

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Chemical Property of trans-dichlorobis(2,2'-bipyridyl-4,4'-dicarboxylic acid)ruthenium(II)

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Technology Process of trans-dichlorobis(2,2'-bipyridyl-4,4'-dicarboxylic acid)ruthenium(II)

There total 1 articles about trans-dichlorobis(2,2'-bipyridyl-4,4'-dicarboxylic acid)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 6813-38-3
2,2'-Bipyridine-4,4'-dicarboxylic acid

: (2E,2’E)-dibutyl 3,3’-(((1E,1’E)-[2,2’-bipyridine]-4,4’-diylbis(ethene-2,1-diyl))bis(2,5-dimethoxy-4,1-phenylene))bis(2-cyanoacrylate)

: 123049-50-3,258352-43-1,73587-30-1
bis(4,4'-dicarboxy-2,2'-bipyridine)dichlororuthenium(II)

: C₅₈H₅₆Cl₂N₆O₁₂Ru

Guidance literature:: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; (2E,2’E)-dibutyl 3,3’-(((1E,1’E)-[2,2’-bipyridine]-4,4’-diylbis(ethene-2,1-diyl))bis(2,5-dimethoxy-4,1-phenylene))bis(2-cyanoacrylate); In N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere; Darkness;

2,2'-Bipyridine-4,4'-dicarboxylic acid; at 160 ℃; for 4h; Inert atmosphere;
DOI:10.1002/asia.201501324

Reference yield: 83.0%

: hexafluorophosphoric acid

: 123049-50-3,258352-43-1,73587-30-1
bis(4,4'-dicarboxy-2,2'-bipyridine)dichlororuthenium(II)

: N-(carboxy-2,3,5,6-tetrafluoro-4-methoxyphenyl)-8-aminoquinoline

: [Ru(dcbpy)₂{(MeOF₄Ph)(N-(carboxyamido)quiniolate)}](PF₆)

Guidance literature:: bis(4,4'-dicarboxy-2,2'-bipyridine)dichlororuthenium(II); N-(carboxy-2,3,5,6-tetrafluoro-4-methoxyphenyl)-8-aminoquinoline; With tetra(n-butyl)ammonium hydroxide; In methanol; at 150 ℃; Inert atmosphere; Sealed tube; Microwave irradiation;

hexafluorophosphoric acid; In water; at 20 ℃; pH=7; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201605991

Reference yield: 72.0%

: hexafluorophosphoric acid

: 123049-50-3,258352-43-1,73587-30-1
bis(4,4'-dicarboxy-2,2'-bipyridine)dichlororuthenium(II)

: 5,7-bis(perfluorophenyl)-8-hydroxyquinoline

: [Ru(dcbpy)₂{5,7-bis(pentafluorophenyl)-8-oxyquinolate}](PF₆)

Guidance literature:: bis(4,4'-dicarboxy-2,2'-bipyridine)dichlororuthenium(II); 5,7-bis(perfluorophenyl)-8-hydroxyquinoline; With tetra(n-butyl)ammonium hydroxide; In methanol; at 150 ℃; Inert atmosphere; Sealed tube; Microwave irradiation;

hexafluorophosphoric acid; In water; at 20 ℃; pH=7; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201605991