2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

Base Information

Chemical Name:2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol
CAS No.:130147-67-0
Molecular Formula:C₃₉H₄₂N₄O₆
Molecular Weight:662.786
Hs Code.:

2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<<N-benzyl-4-carbomethoxybutanamido>methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

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Chemical Property of 2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

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Technology Process of 2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

There total 5 articles about 2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1501-26-4
methyl 4-(chlorocarbonyl)butyrate

: 130147-67-0
2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / pyridine / 1 h / 0 °C

2: 1.2 N HCl / tetrahydrofuran / 0.17 h

3: Et₃N / methanol / 0.08 h / Heating

With pyridine; hydrogenchloride; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jo00313a026

Reference yield:

: 130147-51-2
7-<(benzylamino)methyl>-2,4,6-triphenyl-1,3,5-triazaadamantane

: 130147-67-0
2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / pyridine / 1 h / 0 °C

2: 1.2 N HCl / tetrahydrofuran / 0.17 h

3: Et₃N / methanol / 0.08 h / Heating

With pyridine; hydrogenchloride; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jo00313a026

Reference yield:

: 130147-50-1
7-<(benzylideneamino)methyl>-2,4,6-triphenyl-1,3,5-triazaadamantane

: 130147-67-0
2,2'-<<2-<<<(2-hydroxyphenyl)methylene>amino>methyl>-2-<methyl>-1,3-propanediyl>bis(nitrilomethylidyne)>bisphenol

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / NaBH₄ / CHCl₃; methanol / 2 h / 0 °C

2: 59 percent / pyridine / 1 h / 0 °C

3: 1.2 N HCl / tetrahydrofuran / 0.17 h

4: Et₃N / methanol / 0.08 h / Heating

With pyridine; hydrogenchloride; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jo00313a026