Technology Process of C25H25NO3
There total 6 articles about C25H25NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
toluene;
at 185 ℃;
for 3h;
Microwave irradiation;
DOI:10.1021/jo501231q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water; dichloromethane / 8 h / 20 °C
2: toluene / 3 h / 185 °C / Microwave irradiation
With
tetra-(n-butyl)ammonium iodide; sodium hydroxide;
In
dichloromethane; water; toluene;
DOI:10.1021/jo501231q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bismuth(III) chloride / acetonitrile; water / 24 h / 0 - 24 °C
2: sodium hydrogencarbonate; sodium periodate / water; dichloromethane / 24 h / 25 °C
3: indium; ammonium chloride / water; tetrahydrofuran / 24 h / 0 °C
4: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water; dichloromethane / 8 h / 20 °C
5: toluene / 3 h / 185 °C / Microwave irradiation
With
bismuth(III) chloride; indium; sodium periodate; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; ammonium chloride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
3: |Barbier Coupling Reaction;
DOI:10.1021/jo501231q