N-[2-(1-Cyclopenten-1-yl)-6-methylphenyl]-N'-phenylethanimidamide

Base Information

• Chemical Name: N-[2-(1-Cyclopenten-1-yl)-6-methylphenyl]-N'-phenylethanimidamide
• CAS No.: 407577-56-4
• Molecular Formula: C₂₀H₂₂N₂
• Molecular Weight: 290.408
• DSSTox Substance ID: DTXSID501167341
• Mol file: 407577-56-4.mol

Synonyms:DTXSID501167341;407577-56-4

Chemical Property of N-[2-(1-Cyclopenten-1-yl)-6-methylphenyl]-N'-phenylethanimidamide

Chemical Property:

• XLogP3: 4.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 290.178298710
• Heavy Atom Count: 22
• Complexity: 417

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C(C(=CC=C1)C2=CCCC2)N=C(C)NC3=CC=CC=C3

Technology Process of N-[2-(1-Cyclopenten-1-yl)-6-methylphenyl]-N'-phenylethanimidamide

There total 3 articles about N-[2-(1-Cyclopenten-1-yl)-6-methylphenyl]-N'-phenylethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

6-(cyclopent-1-en-1-yl)-2-methyl-aniline (235779-09-6) + Acetanilid (103-84-4) → 1-phenylamino-1-[2'-methyl-6'-(cyclopent-1-enyl)phenyl-(Z)-imino]ethane (407577-56-4,368430-50-6)

Guidance literature:

With phosphorus pentachloride; In chloroform; at 80 ℃; for 2.5h;

DOI:10.1023/A:1012413715466

Reference yield: 93.0%

6-(cyclopent-1-en-1-yl)-2-methyl-aniline (235779-09-6) + N-phenylimino-1-chloroethane → 1-phenylamino-1-[2'-methyl-6'-(cyclopent-1-enyl)phenyl-(Z)-imino]ethane (407577-56-4,368430-50-6)

Guidance literature:

In benzene; for 2.5h; Heating;

DOI:10.1023/A:1011346231766

Reference yield:

Acetanilid (103-84-4) → 1-phenylamino-1-[2'-methyl-6'-(cyclopent-1-enyl)phenyl-(Z)-imino]ethane (407577-56-4,368430-50-6)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₅ / hexane / 0 °C

2: 93 percent / benzene / 2.5 h / Heating

With phosphorus pentachloride; In hexane; benzene;

DOI:10.1023/A:1011346231766

upstream raw materials:

6-(cyclopent-1-en-1-yl)-2-methyl-aniline

Acetanilid