4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Base Information

Chemical Name:4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole
CAS No.:132142-79-1
Molecular Formula:C₂₃H₂₇NO₂S
Molecular Weight:381.539
Hs Code.:

4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopent<g>indole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Chemical Property:

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Technology Process of 4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

There total 2 articles about 4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132142-68-8,132202-08-5,132202-13-2,132202-14-3
3,5-dimethyl-2-(1-phenylsulfonyl-2-pyrrolyl)cyclopentanone

: 132142-79-1,132142-90-6
4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 15percent BuLi / 1) hexane, Et₂O, -54 to -41 deg C, 1h, 2) toluene, -78 to -63 deg C, 1h

2: 6percent H₂SO₄ / propan-2-ol / 8 h / Heating

With n-butyllithium; sulfuric acid; In isopropyl alcohol;
DOI:10.1016/S0040-4020(01)86755-7

Reference yield:

: (2R,3R)-2-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-1-[2-(dimethyl-hydrazono)-hexyl]-3,5-dimethyl-cyclopentanol

: 132142-80-4
1-[(4S,5R)-5-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,4-dimethyl-cyclopent-1-enyl]-hexan-2-one

: 132142-79-1,132142-90-6
4-(1-butyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Guidance literature:: With sulfuric acid; In isopropyl alcohol; for 8h; Yield given. Yields of byproduct given; Heating;
DOI:10.1016/S0040-4020(01)86755-7