2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene

Base Information

Chemical Name:2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene
CAS No.:1297501-95-1
Molecular Formula:C₃₀H₃₃N₃S₆
Molecular Weight:628.008
Hs Code.:

Synonyms:

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Chemical Property of 2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene

Chemical Property:

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Technology Process of 2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene

There total 7 articles about 2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 2637-34-5,73018-10-7
2-Sulfanylpyridine

: 1297501-89-3
C₁₅H₂₄O₃S₃

: 1297501-95-1
2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene

Guidance literature:: In 1,4-dioxane; at 101 ℃; for 3h;
DOI:10.1055/s-0030-1259306

Reference yield:

: 3BrH*C₁₈H₃₀N₆S₃

: 1297501-95-1
2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water / 4 h / Reflux

2: N-benzyl-trimethylammonium hydroxide / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

4: 40 °C / Heating

5: 1,4-dioxane / 3 h / 101 °C

With N-benzyl-trimethylammonium hydroxide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1055/s-0030-1259306

Reference yield:

: 102-25-0
1,3,5-triethylbenzene

: 1297501-95-1
2,4,6-triethyl-1,3,5-tri-{[(pyridine-2-yl)dithio]methyl}benzene

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogen bromide; zinc dibromide / acetic acid / Reflux

2: ethanol / 20 h / 20 °C

3: sodium hydroxide / water / 4 h / Reflux

4: N-benzyl-trimethylammonium hydroxide / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

6: 40 °C / Heating

7: 1,4-dioxane / 3 h / 101 °C

With hydrogen bromide; N-benzyl-trimethylammonium hydroxide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; zinc dibromide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; acetic acid;
DOI:10.1055/s-0030-1259306