3,3-Dimethylcyclobutanone

Base Information

• Chemical Name: 3,3-Dimethylcyclobutanone
• CAS No.: 1192-33-2
• Molecular Formula: C6H10O
• Molecular Weight: 98.1448
• Hs Code.: 2914299000
• Mol file: 1192-33-2.mol

Synonyms:3.3-Dimethylcyclobutanon;3,3-Dimethylcyclobutanone;Dimethyl-3,3-cyclobutanone;Cyclobutanone,3,3-dimethyl;

Chemical Property of 3,3-Dimethylcyclobutanone

Chemical Property:

• Vapor Pressure: 12.8mmHg at 25°C
• Boiling Point: 124.4oC at 760 mmHg
• Flash Point: 22.4oC
• PSA: 17.07000
• Density: 0.926g/cm3
• LogP: 1.37550

Purity/Quality:

99%, ^*data from raw suppliers

3,3-Dimethylcyclobutan-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3-Dimethylcyclobutanone

There total 9 articles about 3,3-Dimethylcyclobutanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + dimethylketene (598-26-5) → 3,3-dimethylcyclobutan-1-one (1192-33-2)

Guidance literature:

With diethyl ether;

DOI:10.1039/jr9380001211

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2,2-Dimethyl-cyclopropanon (10374-06-8) → 2,2-dimethylcyclobutanone (1192-14-9) + 3,3-dimethylcyclobutan-1-one (1192-33-2)

Guidance literature:

In dichloromethane;

DOI:10.1016/S0040-4020(01)90985-8

Reference yield:

1,1-dimethyl-3-methylenecyclobutane (19037-73-1) → 3,3-dimethylcyclobutan-1-one (1192-33-2)

Guidance literature:

With pyridine; ozone; In dichloromethane;

upstream raw materials:

diazomethane

dimethylketene

2,2-Dimethyl-cyclopropanon

1,1-dimethyl-3-methylenecyclobutane

Downstream raw materials:

2,2-dimethylcyclopropane-1-carboxylic acid

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