5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

Base Information

Chemical Name:5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid
CAS No.:95580-78-2
Molecular Formula:C₁₉H₂₇NO₆
Molecular Weight:365.426
Hs Code.:

5-<Acetyl(ethoxycarbonylmethyl)amino>-3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

Synonyms:

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Chemical Property of 5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

Chemical Property:

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Technology Process of 5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

There total 6 articles about 5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95580-77-1
3-O-Acetyl-5--5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

: 95580-78-2
5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

Guidance literature:: With hydrogen; nickel; In methanol; for 16h; Yield given; Ambient temperature;
DOI:10.1002/jlac.198519850113

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 95580-78-2
5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

Guidance literature:: Multi-step reaction with 6 steps

1: dimethylformamide / 0.5 h

2: H₂ / Pd/C / methanol / 24 h / Ambient temperature

3: pyridine

4: 95 percent / methanolate-solution / 0.25 h

5: 50 percent / pyridine / 14 h / Ambient temperature

6: H₂ / Raney nickel / methanol / 16 h / Ambient temperature

With methanolate; hydrogen; palladium on activated charcoal; nickel; In pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1002/jlac.198519850113

Reference yield:

: {[1-((3aR,5R,6S,6aR)-6-Hydroxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-meth-(Z)-ylidene]-amino}-acetic acid ethyl ester

: 95580-78-2
5--3-O-benzyl-5-desoxy-1,2-O-isopropyliden-α-D-xylofuranosid

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: 95 percent / methanolate-solution / 0.25 h

3: 50 percent / pyridine / 14 h / Ambient temperature

4: H₂ / Raney nickel / methanol / 16 h / Ambient temperature

With methanolate; hydrogen; nickel; In pyridine; methanol;
DOI:10.1002/jlac.198519850113