C₁₁H₁₃N₃O

Base Information

Chemical Name:C₁₁H₁₃N₃O
CAS No.:1304513-30-1
Molecular Formula:C₁₁H₁₃N₃O
Molecular Weight:203.244
Hs Code.:

C<sub>11</sub>H<sub>13</sub>N<sub>3</sub>O

Synonyms:

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Chemical Property of C₁₁H₁₃N₃O

Chemical Property:

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Technology Process of C₁₁H₁₃N₃O

There total 11 articles about C₁₁H₁₃N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1304513-31-2
C₁₉H₂₀N₄O₃

: 1304513-30-1
C₁₁H₁₃N₃O

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 h / 60 °C / Inert atmosphere

2.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 44 h / 20 °C

3.1: sodium periodate / methanol; water / 0.5 h

4.1: tris(2-carboxyethyl)phosphine / water; acetonitrile / pH 7.4 / aq. phosphate buffer; Inert atmosphere

5.1: water; acetonitrile / pH 7.4 / aq. phosphate buffer; Inert atmosphere

6.1: sulfuric acid; sodium nitrite / tetrahydrofuran; water / 1 h / 0 °C

6.2: 0 - 20 °C

7.1: dipyridinium dichromate / dichloromethane / 4 h / 20 °C

8.1: magnesium / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

8.2: 2 h / -78 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; dipyridinium dichromate; tris(2-carboxyethyl)phosphine; sulfuric acid; water; magnesium; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1039/c1cc10222b

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1304513-30-1
C₁₁H₁₃N₃O

Guidance literature:: Multi-step reaction with 11 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.67 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 18 h / 60 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 3 h / -78 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

4.2: 20 h / 60 °C / Inert atmosphere

5.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 44 h / 20 °C

6.1: sodium periodate / methanol; water / 0.5 h

7.1: tris(2-carboxyethyl)phosphine / water; acetonitrile / pH 7.4 / aq. phosphate buffer; Inert atmosphere

8.1: water; acetonitrile / pH 7.4 / aq. phosphate buffer; Inert atmosphere

9.1: sulfuric acid; sodium nitrite / tetrahydrofuran; water / 1 h / 0 °C

9.2: 0 - 20 °C

10.1: dipyridinium dichromate / dichloromethane / 4 h / 20 °C

11.1: magnesium / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

11.2: 2 h / -78 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; dipyridinium dichromate; tris(2-carboxyethyl)phosphine; sulfuric acid; water; diisobutylaluminium hydride; magnesium; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1039/c1cc10222b

Reference yield:

: 23138-53-6
methyl 4-isocyanatobenzoate

: 1304513-30-1
C₁₁H₁₃N₃O

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 18 h / 60 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 3 h / -78 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3.2: 20 h / 60 °C / Inert atmosphere

4.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 44 h / 20 °C

5.1: sodium periodate / methanol; water / 0.5 h

6.1: tris(2-carboxyethyl)phosphine / water; acetonitrile / pH 7.4 / aq. phosphate buffer; Inert atmosphere

7.1: water; acetonitrile / pH 7.4 / aq. phosphate buffer; Inert atmosphere

8.1: sulfuric acid; sodium nitrite / tetrahydrofuran; water / 1 h / 0 °C

8.2: 0 - 20 °C

9.1: dipyridinium dichromate / dichloromethane / 4 h / 20 °C

10.1: magnesium / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

10.2: 2 h / -78 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; dipyridinium dichromate; tris(2-carboxyethyl)phosphine; sulfuric acid; water; diisobutylaluminium hydride; magnesium; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1039/c1cc10222b