Technology Process of C32H40ClCuN3O
There total 7 articles about C32H40ClCuN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
tetrahydrofuran; methanol;
for 16h;
DOI:10.1021/ic500638z
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: n-butyllithium
2.1: toluene-4-sulfonic acid
3.1: n-butyllithium / diethyl ether
4.1: hydrogenchloride / Heating
5.1: oxalyl dichloride / toluene / 16 h / Reflux; Inert atmosphere
5.2: 2 h / Inert atmosphere; Reflux
6.1: titanium tetrachloride / 18 h / 0 °C / Inert atmosphere; Reflux
7.1: sodium methylate / tetrahydrofuran; methanol / 16 h
With
hydrogenchloride; n-butyllithium; oxalyl dichloride; sodium methylate; titanium tetrachloride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; diethyl ether; toluene;
DOI:10.1021/ic500638z
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: toluene-4-sulfonic acid
2.1: n-butyllithium / diethyl ether
3.1: hydrogenchloride / Heating
4.1: oxalyl dichloride / toluene / 16 h / Reflux; Inert atmosphere
4.2: 2 h / Inert atmosphere; Reflux
5.1: titanium tetrachloride / 18 h / 0 °C / Inert atmosphere; Reflux
6.1: sodium methylate / tetrahydrofuran; methanol / 16 h
With
hydrogenchloride; n-butyllithium; oxalyl dichloride; sodium methylate; titanium tetrachloride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; diethyl ether; toluene;
DOI:10.1021/ic500638z
